HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2371990Generated: October 29, 2026
3,5-Dimethoxybenzoyl chloride → HCID 14366289, compound
https://huagongshe.com/reaction/2371990
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3,5-Dimethoxybenzoyl chloride | HCID 87003 | — |
| Reactant | 6-methoxy-(6H)-dibenz[c,e][1,2]-oxaphosphorin | HCID 11436148 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14366289 | HCID 14366289 | — |
Reaction Steps
35.1 g (0.175 mol) of 3,5-dimethoxybenzoyl chloride were warmed to 80° C. under a nitrogen atmosphere. 40.3 g (0.175 mol) of 6-methoxy-(6H)-dibenz[c,e][1,2]oxaphosphorin were added dropwise over the course of one hour while stirring. At the same time, the temperature was gradually increased to 115° C. When the reaction was complete, 60 ml of toluene were added at 80° C. After crystallization, 49 g (74% of theory) of the abovementioned compound of melting point 140° to 142° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05096935 |
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| Source dataset | uspto-grants-1992_03 |
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| ORD ID | ord-3a2506d8d5a542ed9c236a04227451b0 |
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| Source note | uspto-grants-1992_03 |
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