HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2371996Generated: October 30, 2026
1-Naphthalenecarbonyl chloride → HCID 14366294, compound
https://huagongshe.com/reaction/2371996
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Naphthalenecarbonyl chloride | HCID 70146 | — |
| Reactant | 6-methoxy-(6H)-dibenz[c,e][1,2]-oxaphosphorin | HCID 11436148 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14366294 | HCID 14366294 | — |
Reaction Steps
50 g (0.262 mol) of 1-naphthoyl chloride were warmed to 80° to 85° C. under a nitrogen atmosphere. 60.3 g (0.262 mol) of 6-methoxy-(6H)-dibenz[c,e][1,2]oxaphosphorin were added dropwise while stirring. The reaction proceeded exothermically. The temperature was then increased in steps to 125° C. When the reaction was complete, 90 ml of toluene were added at 40° C. After crystallization 77 g (80% of theory) of the abovementioned compound of melting point 149° to 151° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05096935 |
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| Source dataset | uspto-grants-1992_03 |
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| ORD ID | ord-e6fa923e417345928ed2a6984ee0de68 |
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| Source note | uspto-grants-1992_03 |
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