HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19905655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Monobasic potassium phosphate | HCID 516951 | — |
| Reactant | HCID 54448261 | HCID 54448261 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19905655 | HCID 19905655 | 61.4% |
Reaction Steps
A reaction procedure similar to step (2) of Example 1 was followed using 18.8 grams of sodium hydroxide, 13 grams of water, 86 ml of methanol, 50 grams (0.12 mol) of 4,4'-bis[(dimethylmethoxysilyl)methoxy]benzophenone resulting from step (1), 120 ml of ethanol, 18.8 grams of sodium hydroxide, 86 ml of water, 137 grams of potassium dihydrogen phosphate, and 2,200 grams of ice water. Recrystallization from toluene gave 28.8 grams (yield 61%) of pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05096991 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-61aa4bcc12b14d74bc3ed6fb4fe563a8 |
| Source note | uspto-grants-1992_03 |