HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 14514996, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2,3,4,5-Tetrafluoro-6-nitrobenzoic acid | HCID 2733983 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14514996 | HCID 14514996 | — |
Reaction Steps
A solution of 6.7 g (28 mmoles) of 2-nitro-3,4,5,6-tetrafluorobenzoic acid [Tetrahedron, 23, 4719, (1967)], 3.8 g (30 mmoles) of oxalyl chloride and 50 ml of dichloromethane was treated with four drops of N,N-dimethylformamide and stirred at room temperature overnight. The solvent was removed and the residue was used as is without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05097032 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-52db3bd0a2bc4eb4885eff843a0bfe2b |
| Source note | uspto-grants-1992_03 |