5-Bromopentanenitrile → HCID 14820138, compound

HRID 2372274Notes

Reaction equation

HRID 2372274 reaction equation
[CH2:1]([C:3]1[C:4]([OH:18])=[CH:5][C:6]([OH:17])=[C:7]([CH:16]=1)[C:8]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=[O:9])[CH3:2].Br[CH2:20][CH2:21][CH2:22][CH2:23][C:24]#[N:25]>>[C:8]([C:7]1[C:6]([OH:17])=[CH:5][C:4]([O:18][CH2:20][CH2:21][CH2:22][CH2:23][C:24]#[N:25])=[C:3]([CH2:1][CH3:2])[CH:16]=1)(=[O:9])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 794355-BromopentanenitrileHCID 13011871HCID 13011871, compound

Product 1

HCID 14820138HCID 14820138, compoundYield 38.2%

Procedure

Following the procedure of Example 16, 0.726 g of 5-ethyl-2,4-dihydroxybenzophenone and 0.53 g of 5-bromopentanenitrile were allowed to react and provided 0.37 g of the desired title product, m.p. =42°-44° C.

Workup

  1. customto react

Sources & evidence

ORD record
ord-36897998965b4209b54f1cc0d7880c1d
Source dataset
uspto-grants-1992_03
Patent number
US05098613

Reaction notes

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