Dodecanoyl chloride → HCID 19903133, compound

HRID 2372300Notes

Reaction equation

HRID 2372300 reaction equation
[CH2:1]([O:8][CH2:9][CH:10]([OH:13])[CH2:11][OH:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:14](Cl)(=[O:26])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]>>[C:14]([O:12][CH2:11][CH:10]([CH2:9][O:8][CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[O:13][C:14](=[O:26])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])(=[O:26])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]

Participants

3

Reactant 2

HCID 8166Dodecanoyl chlorideHCID 980723-(Benzyloxy)-1,2-propanediol

Product 1

HCID 19903133HCID 19903133, compoundYield 76.2%

Procedure

3-O-Benzylglycerol (7 g) is reacted with 18.5 g of lauroyl chloride in the same manner as in Starting Material Synthesis 2. Recrystallization of the crude crystals from ethanol gives 16 g of white crystals. Melting point: 30°-31° C.

Workup

  1. customMaterial Synthesis 2
  2. customRecrystallization of the crude crystals from ethanol

Sources & evidence

ORD record
ord-bcb0588ff3674970a50c5e6cfaba890e
Source dataset
uspto-grants-1992_03
Patent number
US05098898

Reaction notes

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