HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19903221, compound → HCID 19008878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19903221 | HCID 19903221 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ammonium Hydroxide | HCID 14923 | — |
| Product | HCID 19008878 | HCID 19008878 | 100.5% |
Reaction Steps
A solution of VII (19.0 g, 74.2 mmol) in methanol (150 mL) and ammonium hydroxide (50 mL of a 30% solution) was hydrogenated over a Raney nickel catalyst (ca 5 g) at 60 psi for 30 hr. The mixture was filtered and concentrated in vacuo to give the product as a light green oil (19.40 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05098904 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-dd141c11023a4dc2a2e2ad58283759eb |
| Source note | uspto-grants-1992_03 |