Benzamide → HCID 19904295, compound

HRID 2372406Notes

Reaction equation

HRID 2372406 reaction equation
[CH2:1]1[CH2:12][C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:4](=[O:5])[CH2:3][CH2:2]1.[C:13](N)(=[O:20])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[C:4]12([C:6]3[CH:7]=[CH:8][CH:9]=[CH:10][C:11]=3[CH2:12][CH2:1][CH2:2][CH2:3]1)[C:19]1[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=1)[C:13](=[O:20])[O:5]2

Participants

3

Reactant 2

HCID 2331BenzamideHCID 70003Benzosuberone

Product 1

HCID 19904295HCID 19904295, compound

Procedure

Using a procedure similar to that described in Example 1a except adding 1-benzosuberone to the solution of dilithiated benzamide, the title compound was obtained as a white crystalline solid (46%), mp 150°-151° C. Analysis for C18H16O2 : Calculated: C, 81.79; H, 6.10. Found: C, 81.97; H, 6.08.

Sources & evidence

ORD record
ord-f35e2a174f444772984d57da19d9f59b
Source dataset
uspto-grants-1992_03
Patent number
US05098925

Reaction notes

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