HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethyltetrahydropyran-4-one → 4-(3-Benzyloxyphenyl)-4-hydroxy-2,2-dimethyltetrahydropyran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethyltetrahydropyran-4-one | HCID 1738159 | — |
| Reactant | 1-(Benzyloxy)-3-bromobenzene | HCID 2756638 | — |
| Product | 4-(3-Benzyloxyphenyl)-4-hydroxy-2,2-dimethyltetrahydropyran | HCID 20080653 | 72% |
Reaction Steps
Using the procedure described in the 2nd paragraph of the portion of Example 3 which is concerned with the preparation of starting materials, 3-benzyloxybromobenzene (1.34 g) was reacted with 2,2-dimethyltetrahydropyran-4-one (0.65 g) to give 4-(3-benzyloxyphenyl)-4-hydroxy-2,2-dimethyltetrahydropyran (1.14 g, 72%), as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05098930 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-a35c88aa0c7b498bbe47c33edc36c9f4 |
| Source note | uspto-grants-1992_03 |