HCID 21663940, compound → HCID 53720646, compound

Participants

Reaction Steps

57 mg (0.17 mmol) of diethyl 2-[1-(2-ethoxy)ethoxypent-4-yl]-2-allylmalonate prepared above was dissolved in 10 mL absolute ethanol and combined with 6 mg (56 umol) 10% palladium on carbon. The mixture was flushed with hydrogen and hydrogenated for 4 hrs at 44 psi. Removal of the catalyst by filtration through Celite® brand diatomite and concentration provided 53 mg of a colorless oil.

Provenance & Evidence