Oxygen → 4-(3,7,11,15-tetramethyl-6,10,14-hexadecatrienoyl)morpholine

HRID 2372575Notes

Reaction equation

O=O.[C:3]([C:7]1[CH:12]=[CH:11][CH:10]=[C:9]([C:13]([CH3:16])([CH3:15])[CH3:14])[C:8]=1O)([CH3:6])([CH3:5])[CH3:4].[OH-:18].[K+].[OH-:20].[Na+]>>[C:3]([C:7]1[CH:12]=[C:11]([OH:20])[CH:10]=[C:9]([C:13]([CH3:16])([CH3:15])[CH3:14])[C:8]=1[C:8]1[C:7]([C:3]([CH3:5])([CH3:4])[CH3:6])=[CH:12][C:11]([OH:18])=[CH:10][C:9]=1[C:13]([CH3:16])([CH3:15])[CH3:14])([CH3:6])([CH3:5])[CH3:4]

Participants

Reactant 4

HCID 977Oxygen

HCID 14797Potassium Hydroxide

HCID 14798Sodium Hydroxide

HCID 314052,6-Di-tert-butylphenol

Product 1

HCID 1696244-(3,7,11,15-tetramethyl-6,10,14-hexadecatrienoyl)morpholine

Procedure

oxidizing the resulting reaction liquid using oxygen without isolating said 2,6-di-t-butyl phenol from the liquid in the presence of KOH or NaOH as an alkaline catalyst to produce 3,3',5,5'-tetra-t-butyl-4,4'-biphenol,

Workup

customthe resulting reaction liquid
customwithout isolating

Sources & evidence

ORD record: ord-982a407ef00b4b74a48173e4b94d632c
Source dataset: uspto-grants-1992_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05099076

Reaction notes

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