HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-(Chlorocarbonyl)phenyl nonanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(Nonanoyloxy)benzoic acid | HCID 3563821 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 4-(Chlorocarbonyl)phenyl nonanoate | HCID 13531043 | — |
Reaction Steps
2.5 g of 4-octylcarbonyloxybenzoic acid was dispersed in 50 ml carbon tetrachloride, after dropping 10 ml of thionyl chloride to this solution, refluxed for three hours. After reducing the solvent, 4-octylcarbonyloxybenzoic chloride (CK) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05100579 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-9798d60ffc9a4a22a11c8ca7d6213637 |
| Source note | uspto-grants-1992_03 |