HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15045704, compound → HCID 15045705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15045704 | HCID 15045704 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 15045705 | HCID 15045705 | — |
Reaction Steps
0.1 mole 2-Hydroxy-5-formylbenzylphosphonic acid diethyl ester was refluxed for 3 hours with 100 ml 6N HCl. Product was separated out while it was being formed. The reaction solution was cooled in the refrigerator and the product was isolated on a buchner funnel and washed with cold water. mp 252°-253° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05100654 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-92409018059b4718bf463f144527a363 |
| Source note | uspto-grants-1992_03 |