Triethyl phosphite → HCID 15045720, compound

Participants

Reaction Steps

4-Butoxy-3-chloromethylbenzaldehyde and triethyl phosphite in a 1:1 ratio were heated until no more gas evolved and the reaction mixture had turned light orange. The reaction mixture was then vacuum distilled to give the desired product. bp 188° C. at 1.4 mm Hg.

Provenance & Evidence