Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2372686Generated: October 30, 2026

Vinylidene fluoride → HCID 131717214, compound

https://huagongshe.com/reaction/2372686

Reaction equation

Participants

RoleNameHCIDCharge
ReactantVinylidene fluorideHCID 6369—
ReactantMethyl MethacrylateHCID 6658—
ReactantFluoride IonHCID 28179—
Reactant6-Formyl-4,6',7'-trihydroxy-2',5',5',8'a-tetramethyl-3',4',4'a,5',6',7',8',8'a-octahydro-2'H,3H-spiro[1-benzofuran-2,1'-naphthalene]-7-carboxylic acidHCID 119528—
ProductHCID 131717214HCID 131717214—

Reaction Steps

Carrier particles were prepared by coating 150 pounds of a Toniolo atomized steel core, 120 microns in diameter, with 0.45 pounds of polymethyl methacrylate, PMMA, available from Soken Chemical as MP116, and 0.45 pound of polyvinylindene fluoride, available as Kynar 301F. The core and PMMA are mixed first in a MX-1 Munson mixer for 10 minutes, the mixer is inactivated, the Kynar added and mixing continued for 20 more minutes. There results an electrostatically attached uniform distribution of the Kynar/PMMA on the carrier core as determined by visual observation. The resulting carrier particles were metered into a rotating tube furnace available from Harper Company at a rate of 400 grams/minute. This furnace was maintained at a temperature of 400° F. thereby causing the polymers to melt and fuse to the core.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05100753
Source datasetuspto-grants-1992_03
ORD IDord-ce614f5fe9424195ba7e7f486b4aa8ee
Source noteuspto-grants-1992_03