Benzoyl chloride → HCID 20757649, compound

Participants

Role	Name	HCID	Charge
Reactant	Benzoyl chloride	HCID 7412	—
Reactant	Valeryl chloride	HCID 61186	—
Reactant	(4-{[Benzyl({[3,5-bis(trifluoromethyl)benzoyl]amino}sulfonyl)amino]methyl}cyclohexyl)methyl benzoate	HCID 22574465	—
Product	HCID 20757649	HCID 20757649	—

Reaction Steps

Following procedure to make (5), valeryl chloride was substituted for benzoyl chloride to give the title compound after purification. 1H NMR (500 MHz, DMSO-d6): δ 8.45 (s, 2H), 8.14 (s, 1H), 7.36 (d, 2H), 7.25 (t, 2H), 7.17 (t, 1H), 4.38 (s, 2H), 3.70 (d, 2H), 3.30 (water), 2.917 (d, 2H), 2.48 (DMSO), 2.22 (t, 2H), 1.62 (m, 2H), 1.52 (m, 2H), 1.45 (m, 2H), 1.37 (m, 1H), 1.26 (m, 1H), 1.22 (m, 2H), 0.82 (t, 3H), 0.63 (m, 4H).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06852738B2
Source dataset	uspto-grants-2005_02
ORD ID	ord-d6f2eef6b0f444038a9660dc991fff7e
Source note	uspto-grants-2005_02