HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 86744010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 86744011 | HCID 86744011 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86744010 | HCID 86744010 | 91% |
Reaction Steps
181 g of methyl 3-chloroalanine hydrochloride were heated under reflux with 163.9 g of acetyl chloride in 1.5 l of anhydrous toluene for about 5 hours until a clear solution was obtained. This was evaporated to dryness and the residue was crystallized from ethyl acetate/petroleum ether. 170 g of product of m.p. 104° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05101039 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-804da394aed949e490da36bc3f781b6f |
| Source note | uspto-grants-1992_03 |