Toluene → HCID 86745609, compound

Participants

Reaction Steps

A solution of 3 g of triethylamine in 89 g of tetrahydrofuran was added dropwise to a mixture of 870 g of toluene, 443 g of tetrahydrofuran, 90 g of 4-hydroxyphenyldimethylsulfonium hexafluorophosphate and 51 g of isocyanatoethyl methacrylate at from 20 to 25° C. in the course of 10 minutes, at a rate such that there was no marked temperature increase After 12 hours, the product was filtered off under suction, washed with toluene and recrystallized from ethanol. Yield: 112 g (82%) of colorless crystals of melting point 102°-104° C.

Provenance & Evidence