HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyanophenol → O-3-cyanophenyl dimethylthiocarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyanophenol | HCID 13394 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| Product | O-3-cyanophenyl dimethylthiocarbamate | HCID 14795402 | — |
Reaction Steps
If the procedure described in Preparation XI is followed starting from 15 g (126.10-3 mol) of 3-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (132.10-3 mol) of potassium hydroxide, 29 g (quantitative yield) of the expected product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05101048 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-87ff7015c4e34deb8be2f93ca8168df5 |
| Source note | uspto-grants-1992_03 |