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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2372967Generated: October 25, 2026

2-Hydroxybenzonitrile → O-2-cyanophenyl dimethylthiocarbamate

https://huagongshe.com/reaction/2372967

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-HydroxybenzonitrileHCID 11907—
ReactantPotassium HydroxideHCID 14797—
ReactantDimethylthiocarbamoyl chlorideHCID 27871—
ProductO-2-cyanophenyl dimethylthiocarbamateHCID 1479540394%

Reaction Steps

If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05101048
Source datasetuspto-grants-1992_03
ORD IDord-62a3c0ac533743b5b3990520ae9c3fb3
Source noteuspto-grants-1992_03