HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → 3,5-Dicyano-2-mercaptobenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | 2-Bromobenzene-1,3,5-tricarbonitrile | HCID 12575939 | — |
| Product | 3,5-Dicyano-2-mercaptobenzonitrile | HCID 14795337 | — |
Reaction Steps
If the procedure described in Preparation LV is followed starting from 6 g (26.10-3 mol) of 2-bromo-3,5-dicyanobenzonitrile and 6 g (86.10-3 mol) of sodium thiomethylate, 6 g (quantitative yield) of the expected product are obtained in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05101048 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-0be296470203476582048edd0b81c4af |
| Source note | uspto-grants-1992_03 |