Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Methoxide → HCID 15067863, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 반응물 | 4-acetamidophenyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 15067862 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 15067863 | HCID 15067863 | 83% |
반응 단계
If the procedure described in Preparation LXXXIV is followed starting from 1.2 g (2.8.10-3 mol) of 4-acetamidophenyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside and 70 μl of a solution of sodium methylate in methanol (8% w/v of Na), reacted in 100 cm3 of methanol, 0.7 g (yield: 83%) of the expected product is obtained after purification by flash chromatography using a methylene chloride/methanol mixture (93/7 v/v) as the eluent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05101048 |
| 출처 데이터셋 | uspto-grants-1992_03 |
| ORD ID | ord-f074db355aab4ac8a3d2f1bb3bb1b8f3 |
| 출처 메모 | uspto-grants-1992_03 |