4-Nitrobenzaldehyde → HCID 67897623, compound

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Reaction Steps

p-Nitrobenzaldehyde is reacted with acetophenone and sodium hydroxide in ethanol to produce 3-(p-nitrophenyl)-3-hydroxy-1-phenyl propanone. The resulting compound is reacted with KHSO4 to obtain p-nitrochalcone. p-Nitrochalcone is hydrogenated in the presence of platinum catalyst to produce 3-(p-aminophenyl)-1-phenyl propanone. The resulting compound is reacted with potassium hydroxide and hydrazine in triethylene glycol to produce p-aminodiophenylpropane. p-Aminodiphenylpropane is reacted with fuming nitric acid and acetic acid anhydride to obtain 1-(p-aminophenyl)-3-p-nitrophenyl)-propane.

Provenance & Evidence