HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 1-Benzyl-8-chloro-3,4-dihydro-1H-benzo[b]azepine-2,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 11390173 | HCID 11390173 | — |
| Product | 1-Benzyl-8-chloro-3,4-dihydro-1H-benzo[b]azepine-2,5-dione | HCID 66934675 | 38% |
Reaction Steps
In a manner similar to that described for Method W, 8-chloro-3,4-dihydro-1H-benzo[b]azepine-2,5-dione and benzyl bromide were converted to the title compound (38%): MS m/z═300 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459448B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-8956a25c945b4ec4b773896b5a8efeed |
| Source note | uspto-grants-2008_12 |