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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2373367Generated: October 30, 2026

8-chloro-4-dimethylaminomethylene-1-methyl-3,4-dihydro-1H-benzo[b]azepine-2,5-dione → HCID 59851940, compound

https://huagongshe.com/reaction/2373367

Reaction equation

Participants

RoleNameHCIDCharge
Reactant8-chloro-4-dimethylaminomethylene-1-methyl-3,4-dihydro-1H-benzo[b]azepine-2,5-dioneHCID 66934686—
ReactantHCID 178512548HCID 178512548—
ProductHCID 59851940HCID 59851940—

Reaction Steps

In a manner similar to that described for method I, 8-chloro-4-dimethylaminomethylene-1-methyl-3,4-dihydro-1H-benzo[b]azepine-2,5-dione (v-m) and 4-guanidinobenzoic acid were converted to I-7 (30%): HRMS Calcd. for C20H15ClN4O3: 395.0910, Found 395.0923.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07459448B2
Source datasetuspto-grants-2008_12
ORD IDord-f28af82618f646cf8f42f4ed00cc5cfd
Source noteuspto-grants-2008_12