huagongshe.com
HRID2373369

反应详情

EQUATION

反应方程式

HRID 2373369 的结构方程式

REACTANTS

反应物

2
结构：CC1C(=O)N(C)c2cc(Cl)ccc2C(=O)C1=CN(C)C
HCID66934671

未命名化合物

结构：N=C(N)Nc1ccc(C(=O)O)cc1
HCID178512548

未命名化合物

PRODUCTS

生成物

1
结构：CC1C(=O)N(C)c2cc(Cl)ccc2-c2nc(Nc3ccc(C(=O)O)cc3)ncc21
HCID57663153

未命名化合物

PROCEDURE

实验过程

In a manner similar to that described for method I, 8-chloro-4-dimethylaminomethylene-1,3-dimethyl-3,4-dihydro-1H-benzo[b]azepine-2,5-dione (v-o) and 4-guanidinobenzoic acid were converted to I-68 (6%) after purification by C-18 RP LC-MS chromatography: HRMS Calcd. for C21H17ClN4O3: 409.1067, Found 409.1052.

WORKUP

后处理

  1. customafter purification by C-18 RP LC-MS chromatography