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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2373422Generated: October 30, 2026

8-chloro-4-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dione → HCID 56946586, compound

https://huagongshe.com/reaction/2373422

Reaction equation

Participants

RoleNameHCIDCharge
Reactant8-chloro-4-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dioneHCID 66934877—
ReactantHCID 178512495HCID 178512495—
ProductHCID 56946586HCID 56946586—

Reaction Steps

In a manner similar to method I, 8-chloro-4-((dimethylamino)methylene)-3,4-dihydro-1H-benzo[b]azepine-2,5-dione (v-j) and 3-guanidino-benzoic acid were converted to I-62-a (72%): MS m/z═381 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07459448B2
Source datasetuspto-grants-2008_12
ORD IDord-f45a0b9e474f4d708e1c4b4d42334f5b
Source noteuspto-grants-2008_12