HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11462234, compound → HCID 69292336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11462234 | HCID 11462234 | — |
| Reactant | (4-Ethynylphenyl)(morpholino)methanone | HCID 57764578 | — |
| Reactant | 7-iodo-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine | HCID 59852691 | — |
| Product | HCID 69292336 | HCID 69292336 | — |
Reaction Steps
The title compound is prepared in analogy to 3-(3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepin-7-ylethynyl)-benzoic acid ethyl ester (10) from (4-ethynyl-phenyl)-morpholin-4-yl-methanone and 7-iodo-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine (5) as a yellow viscous oil, MS (ESI) 392.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459480B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-f25069baada2450995a3be298d056422 |
| Source note | uspto-grants-2008_12 |