4-(Methylthio)phenol → HCID 69292339, compound

HRID 2373467Notes

Reaction equation

HRID 2373467 reaction equation
[CH3:1][C:2]1([CH3:15])[CH2:8][O:7][C:6]2[CH:9]=[CH:10][C:11]([CH2:13][OH:14])=[CH:12][C:5]=2[O:4][CH2:3]1.[CH3:16][S:17][C:18]1[CH:23]=[CH:22][C:21](O)=[CH:20][CH:19]=1>>[CH3:1][C:2]1([CH3:15])[CH2:8][O:7][C:6]2[CH:9]=[CH:10][C:11]([CH2:13][O:14][C:21]3[CH:22]=[CH:23][C:18]([S:17][CH3:16])=[CH:19][CH:20]=3)=[CH:12][C:5]=2[O:4][CH2:3]1

Participants

3

Reactant 2

HCID 140864-(Methylthio)phenolHCID 59852696HCID 59852696, compound

Product 1

HCID 69292339HCID 69292339, compound

Procedure

According to the method described in example 23, the title compound is prepared from (3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepin-7-yl)-methanol (31) and 4-(methylthio)phenol. MS (ESI) 331.3 (M+H)+.

Sources & evidence

ORD record
ord-bafbdc7410bc4d66aa6238be9fb04ab0
Source dataset
uspto-grants-2008_12
Patent number
US07459480B2

Reaction notes

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