4-Methoxyphenol → HCID 69292921, compound

HRID 2373468Notes

Reaction equation

HRID 2373468 reaction equation
[CH3:1][C:2]1([CH3:15])[CH2:8][O:7][C:6]2[CH:9]=[CH:10][C:11]([CH2:13][OH:14])=[CH:12][C:5]=2[O:4][CH2:3]1.[CH3:16][O:17][C:18]1[CH:23]=[CH:22][C:21](O)=[CH:20][CH:19]=1>>[CH3:16][O:17][C:18]1[CH:23]=[CH:22][C:21]([O:14][CH2:13][C:11]2[CH:10]=[CH:9][C:6]3[O:7][CH2:8][C:2]([CH3:15])([CH3:1])[CH2:3][O:4][C:5]=3[CH:12]=2)=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 90154-MethoxyphenolHCID 59852696HCID 59852696, compound

Product 1

HCID 69292921HCID 69292921, compound

Procedure

According to the method described in example 23, the title compound is prepared from (3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepin-7-yl)-methanol (31) and 4-methoxyphenol. MS (ESI) 332.3 (M+NH4)+.

Sources & evidence

ORD record
ord-7b271b75d3284b049818d2aaf82835ee
Source dataset
uspto-grants-2008_12
Patent number
US07459480B2

Reaction notes

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