HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 5-methoxyindole-2-carboxylate → HCID 21964306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 5-methoxyindole-2-carboxylate | HCID 20926 | — |
| Reactant | 1-(Bromomethyl)-4-(1,1-dimethylethyl)benzene | HCID 87836 | — |
| Product | HCID 21964306 | HCID 21964306 | — |
Reaction Steps
The title compound was prepared from ethyl 5-methoxy-1H-indole-2-carboxylate and 4-(tert-butyl) benzyl bromide in substantially the same manner, as described in step 1 of Example 1. The product was obtained as a solid. Mass spectrum (ESI, [M−H]−) m/z 364. 1H NMR (400 MHz, DMSO-d6) δ 7.48 (d, 1H, J=9.20 Hz), 7.27 (s, 1H), 7.24 (d, 2H, J=7.18 Hz), 7.16 (d, 1H, J=2.44 Hz), 6.96-6.92 (m, 3H), 5.77 (s, 2H), 4.28 (q, 2H), 3.76 (s, 3H), 1.28 (s, 3H), and 1.20 ppm (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459478B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-822a339f414f41e69e321f37542fae07 |
| Source note | uspto-grants-2008_12 |