Methanesulfonyl chloride → 2-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

HRID 2373645Notes

Reaction equation

HRID 2373645 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[CH2:5][CH2:6][OH:7].[CH3:11][S:12](Cl)(=[O:14])=[O:13]>>[CH3:11][S:12]([O:7][CH2:6][CH2:5][C:4]1[CH:8]=[CH:9][CH:10]=[C:2]([NH:1][S:12]([CH3:11])(=[O:14])=[O:13])[CH:3]=1)(=[O:14])=[O:13]

Participants

3

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 149389872-(3-Aminophenyl)ethan-1-ol

Product 1

HCID 574443592-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

Procedure

The title compound was prepared from 3-aminophenethyl alcohol (U.S. Pat. No. 2,641,602) and methanesulfonyl chloride (2 eq.) according to the procedure contained within description 4. The product was used immediately without further purification or characterisation.

Workup

  1. customThe product was used immediately without further purification or characterisation

Sources & evidence

ORD record
ord-2aaf6d071608465eb2da6be343354c6d
Source dataset
uspto-grants-2008_12
Patent number
US07459456B2

Reaction notes

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