3-Acetoxy-2-naphthoic acid → HCID 59852599, compound

HRID 2373826Notes

Reaction equation

HRID 2373826 reaction equation
[C:1]([O:4][C:5]1[C:6]([C:15]([OH:17])=O)=[CH:7][C:8]2[C:13]([CH:14]=1)=[CH:12][CH:11]=[CH:10][CH:9]=2)(=[O:3])[CH3:2].[CH3:18][O:19][C:20]1[C:25]([C:26]2[CH:31]=[CH:30][C:29]([N+:32]([O-:34])=[O:33])=[CH:28][CH:27]=2)=[CH:24][C:23]([CH2:35][CH2:36][NH2:37])=[CH:22][CH:21]=1>>[CH3:18][O:19][C:20]1[C:25]([C:26]2[CH:31]=[CH:30][C:29]([N+:32]([O-:34])=[O:33])=[CH:28][CH:27]=2)=[CH:24][C:23]([CH2:35][CH2:36][NH:37][C:15]([C:6]2[C:5]([O:4][C:1](=[O:3])[CH3:2])=[CH:14][C:13]3[C:8]([CH:7]=2)=[CH:9][CH:10]=[CH:11][CH:12]=3)=[O:17])=[CH:22][CH:21]=1

Participants

3

Reactant 2

HCID 2320383-Acetoxy-2-naphthoic acidHCID 69208050HCID 69208050, compound

Product 1

HCID 59852599HCID 59852599, compound

Procedure

Acetic acid 3-[2-(6-methoxy-4′-nitro-biphenyl-3-yl)-ethylcarbamoyl]-naphthalen-2-yl ester (108 mg) was prepared from 3-Acetoxy-naphthalene-2-carboxylic acid (58 mg, 0.25 mmol) and 2-(6-Methoxy-4′-nitro-biphenyl-3-yl)-ethylamine (68 mg, 0.25 mmol following the general procedure A.

Sources & evidence

ORD record
ord-9edeae5b37a94032a94a80a4086521fe
Source dataset
uspto-grants-2008_12
Patent number
US07459472B2

Reaction notes

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