HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilic Acid → HCID 11771311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilic Acid | HCID 227 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-tert-Butylbenzoyl chloride | HCID 74372 | — |
| Product | HCID 11771311 | HCID 11771311 | 59.9% |
Reaction Steps
The 2-aminobenzoic acid (137 mg, 1.0 mmol) was reacted with 4-tert-butyl benzoyl chloride (196 mg, 1.0 mmol) as described in general procedure M. The resulting compound was coupled with methylamine (62 mg, 2.0 mmol) as described in general procedure A to afford the title product (186 mg) as a pure white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459472B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-e5cdebac56bb4c948b3bdd84006540ef |
| Source note | uspto-grants-2008_12 |