2-Chloro-5-nitrobenzoic acid → HCID 26959384, compound

HRID 2374254Notes

Reaction equation

HRID 2374254 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([C:14](=[O:16])[CH3:15])[CH:5]=[CH:6][C:7]=1[N:8]1[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]1.[Cl:17][C:18]1[CH:26]=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][C:19]=1[C:20](O)=[O:21]>>[Cl:17][C:18]1[CH:26]=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][C:19]=1[C:20]([N:11]1[CH2:12][CH2:13][N:8]([C:7]2[CH:6]=[CH:5][C:4]([C:14](=[O:16])[CH3:15])=[CH:3][C:2]=2[F:1])[CH2:9][CH2:10]1)=[O:21]

Participants

3

Reactant 2

HCID 172872-Chloro-5-nitrobenzoic acidHCID 6856101-(3-Fluoro-4-piperazin-1-ylphenyl)ethanone

Product 1

HCID 26959384HCID 26959384, compound

Procedure

The title compound was prepared according to the procedure D described for example 2 from 1-(3-Fluoro-4-piperazin-1-yl-phenyl)-ethanone and 2-chloro-5-nitro-benzoic acid (CAS: 2516-96-3); MS (ISP): 406.2 MH+.

Sources & evidence

ORD record
ord-bd72816aa6cb44558d04ce6a52b95d5f
Source dataset
uspto-grants-2008_12
Patent number
US07462617B2

Reaction notes

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