Furan, 2-(bromomethyl)tetrahydro- → 2-((4-Bromo-3,5-dimethylphenoxy)methyl)tetrahydrofuran

HRID 237441Notes

Reaction equation

HRID 237441 reaction equation
[Br:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([OH:9])=[CH:4][C:3]=1[CH3:10].Br[CH2:12][CH:13]1[CH2:17][CH2:16][CH2:15][O:14]1>>[Br:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([O:9][CH2:12][CH:13]2[CH2:17][CH2:16][CH2:15][O:14]2)=[CH:4][C:3]=1[CH3:10]

Participants

3

Reactant 2

HCID 14501Furan, 2-(bromomethyl)tetrahydro-HCID 819704-Bromo-3,5-dimethylphenol

Product 1

HCID 866971092-((4-Bromo-3,5-dimethylphenoxy)methyl)tetrahydrofuran

Procedure

The title compound is prepared from 4-bromo-3,5-dimethylphenol and 2-(bromomethyl)tetrahydrofuran following a procedure analogous to that described in Step 3 of Intermediate 2. LC (method 1): tR=1.37 min; Mass spectrum (ESI+): m/z=285 [M+H]+.

Sources & evidence

ORD record
ord-ee837e2e06dd4b118cf671e3ba95d661
Source dataset
uspto-grants-2014_02
Patent number
US08642585B2

Reaction notes

Loading…