HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorovaleryl chloride → HCID 21886968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Reactant | 5,6-Dihydro-4H-pyrrolo[3,2,1-ij]quinolin-2(1H)-one | HCID 14918493 | — |
| Product | HCID 21886968 | HCID 21886968 | 64.9% |
Reaction Steps
Using 5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-2(1H)-one (3.46 g) and 5-chlorovaleryl chloride (3.4 g) according to the same method as that of Reference Example 1, the title compound (3.78 g) was obtained as pale yellow crystals having a melting point of 89 to 90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07462628B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-2abf52299bcc473b92ef76888235fab7 |
| Source note | uspto-grants-2008_12 |