化工社化工社 化学情報印刷レポート · 研究参考用
5-Chlorovaleryl chloride → 9-(5-chloropentanoyl)-1,2,6,7-tetrahydropyrido[3,2,1-ij]quinolin-3(5H)-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Chlorovaleryl chloride | HCID 74089 | — |
| 反応物 | 1,2,6,7-tetrahydro-5H-pyrido[3,2,1-ij]quinolin-3-one | HCID 13694564 | — |
| 生成物 | 9-(5-chloropentanoyl)-1,2,6,7-tetrahydropyrido[3,2,1-ij]quinolin-3(5H)-one | HCID 21887259 | — |
反応手順
Using 2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one and 5-chlorovaleryl chloride according to the same method as that of Reference Example 1, the title compound (3.53 g) was obtained as colorless crystals, having a melting point of 83-84° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07462628B2 |
| 出典データセット | uspto-grants-2008_12 |
| ORD ID | ord-63ff60812e0e4418899874467087897a |
| 出典メモ | uspto-grants-2008_12 |