HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorovaleryl chloride → HCID 21886856, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Reactant | 1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one | HCID 231553 | — |
| Product | HCID 21886856 | HCID 21886856 | 70.7% |
Reaction Steps
Using 1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one (3.00 g) and 5-chlorovaleryl chloride (5.74 g) according to the same method as that of Reference Example 1, the title compound (3.67 g) was obtained as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07462628B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-bffd106f87064bdeaeef6bc5207a6f23 |
| Source note | uspto-grants-2008_12 |