4-Bromo-3,5-dimethylphenol → HCID 86697123, compound

HRID 237458Notes

Reaction equation

HRID 237458 reaction equation
CC1C=CC(S([O:11][CH:12]2[CH2:16][CH2:15][CH:14]([OH:17])[CH2:13]2)(=O)=O)=CC=1.[Br:18][C:19]1[C:24]([CH3:25])=[CH:23][C:22](O)=[CH:21][C:20]=1[CH3:27]>>[Br:18][C:19]1[C:24]([CH3:25])=[CH:23][C:22]([O:11][CH:12]2[CH2:16][CH2:15][CH:14]([OH:17])[CH2:13]2)=[CH:21][C:20]=1[CH3:27]

Participants

3

Reactant 2

HCID 819704-Bromo-3,5-dimethylphenolHCID 58597012HCID 58597012, compound

Product 1

HCID 86697123HCID 86697123, compound

Procedure

The title compound is prepared from 3-hydroxycyclopentyl 4-methylbenzenesulfonate and 4-bromo-3,5-dimethylphenol following a procedure analogous to that described in Step 3 of Intermediate 2. LC (method 7): tR=1.07 min; Mass spectrum (ESI+): m/z=285 [M+H]+.

Sources & evidence

ORD record
ord-40d1f7c9a9104547a062b30101e9c8ce
Source dataset
uspto-grants-2014_02
Patent number
US08642585B2

Reaction notes

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