HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorovaleryl chloride → 5-Chloro-1-(2,2-dimethyl-3,4-dihydro-2H-chromen-6-yl)-1-pentanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Reactant | 2,2-Dimethylchroman | HCID 136936 | — |
| Product | 5-Chloro-1-(2,2-dimethyl-3,4-dihydro-2H-chromen-6-yl)-1-pentanone | HCID 21887307 | — |
Reaction Steps
Using 2,2-dimethylchroman (19.7 g) and 5-chlorovaleryl chloride (20.7 g) according to the same method as that of Reference Example 1, the title compound was obtained as colorless crystals (22.0 g) having a melting point of 50 to 51° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07462628B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-14020e71b0204c938be912d3217a1ce5 |
| Source note | uspto-grants-2008_12 |