Potassium Carbonate → HCID 59853912, compound

Participants

Reaction Conditions

Reaction Steps

150 mg (0.406 mmol) of 2-[4-(5H -dibenzo[a,d][7]annulen-5-ylidene)-1-piperidinyl]-2-oxoethanamine hydrochloride, 80.5 mg (0.406 mmol) of 2,2-dimethyl-1-iodopropane and 84.3 mg (0.610 mmol) of potassium carbonate were dissolved in 1 ml of N,N-dimethylformamide, and the obtained solution was stirred at 120° C. overnight. The product was purified by the silica gel chromatography (hexane: ethyl acetate=9:1 to 2:3) to obtain the title compound.

Provenance & Evidence