HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 58711952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 58711967 | HCID 58711967 | — |
| Reactant | HCID 68870503 | HCID 68870503 | — |
| Product | HCID 58711952 | HCID 58711952 | 83.4% |
Reaction Steps
In a similar manner as described for Intermediate 59, using 1-[3-(Methylthio)-1,2,4-triazin-6-yl]ethanamine (Intermediate 4) (1.00 g, 5.90 mmol), benzoyl chloride (0.75 mL, 6.50 mmol), to give N-{1-[3-(methylthio)-1,2,4-triazin-6-yl]ethyl}benzamide (1.35 g) as a yellow solid. MS m/z 275 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07462614B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-5b1626b02780440ebc5f7525db88d450 |
| Source note | uspto-grants-2008_12 |