HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 137241990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 136181670 | HCID 136181670 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 137241990 | HCID 137241990 | 91% |
Reaction Steps
Preparation of example 32 from the title compound of Example 30 (31 mg, 0.062 mmol) and 45% TFA in CH2Cl2 (1 mL) was carried out analogously to Example 20. Isolation, also in an analogous manner, afforded the title compound (29 mg, 0.056 mmol) as a yellow powder in 91% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07462713B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-6f186c95471e49609b3406c265875bea |
| Source note | uspto-grants-2008_12 |