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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2375106Generated: November 2, 2026

Hydrochloric Acid → HCID 136401945, compound

https://huagongshe.com/reaction/2375106

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 136181609HCID 136181609—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 136401945HCID 136401945100%

Reaction Steps

Preparation of example 177 from the title compound of Example 159 (35 mg, 0.072 mmol) and 4M HCl in dioxane (10 mL) was carried out analogously to Example 91. Isolation, also in an analogous manner afforded the title compound (30 mg, 0.072 mmol) as an orange/yellow powder in 100% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07462713B2
Source datasetuspto-grants-2008_12
ORD IDord-f997fb6317fd49e7a74eca70307a145b
Source noteuspto-grants-2008_12