HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 86606163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | HCID 11327963 | HCID 11327963 | — |
| Product | HCID 86606163 | HCID 86606163 | 67.8% |
Reaction Steps
An ethanolic solution of 0.5 g (1.15 mmol) of sulfone 1 and 0.15 g (1.38 mmol) of phenylhydrazine was refluxed for 14 hours. Cooling, distillative removal of the solvent and chromatography on silica gel (cyclohexane:methyl tert-butyl ether [MTBE] 95:5) gave 0.36 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465735B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-8443148e22cf4a2497315802f00fcdf7 |
| Source note | uspto-grants-2008_12 |