Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Pyridine, 5-ethyl-2-vinyl- | HCID 222462 | — |
| Reactant | Potassium Bromide | HCID 253877 | — |
| Product | HCID 45095769 | HCID 45095769 | 86% |
Reaction Steps
5.5 g (0.0344 mol) liq. Bromine was added to a solution of 7.83 g (0.0658 mol) KBr dissolved in 100 mL water. Reaction mixture was heated to 60-65° C. and 5 g (0.0376 mol) of 5-ethyl-2-vinyl-pyridine was added into it in 10 min. Reaction mixture was stirred for 30 min. and quenched with excess of water. Product was extracted with dichloromethane, which was separated, dried, concentrated and purified to get 7.43 g (86%) of the titled product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07465801B2 |
|---|
| Source dataset | uspto-grants-2008_12 |
|---|
| ORD ID | ord-a2bf36dbc8f64124b008152d897e73de |
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| Source note | uspto-grants-2008_12 |
|---|
