1,3,2-Dioxaborolane, 2-(3-chlorophenyl)- → HCID 11390553, compound
Reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([B:8]2[O:12][CH2:11][CH2:10]O2)[CH:5]=[CH:6][CH:7]=1.Br[C:14]1[CH:19]=[CH:18]C=[CH:16][C:15]=1COCOC>>[Cl:1][C:2]1[CH:3]=[C:4]([B:8]2[C:16]3[CH:15]=[CH:14][CH:19]=[CH:18][C:10]=3[CH2:11][O:12]2)[CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
This was prepared as per the procedure in Example 11, from 2-(3-chlorophenyl)-[1,3,2]-dioxaborolane and 1-bromo-2-((methoxymethoxy)methyl)benzene to afford white crystalline product.
Workup
- customto afford white crystalline product
Sources & evidence
- ORD record
- ord-31f8a7e82e004a6ca95318860c9583f1
- Source dataset
- uspto-grants-2008_12
- Patent number
- US07465836B2
Reaction notes
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