1-Bromo-2-((methoxymethoxy)methyl)benzene → HCID 11218256, compound

HRID 2375774Notes

Reaction equation

HRID 2375774 reaction equation
[C:1]([C:3]1[CH:4]=[C:5]([B:9]2[O:13][CH2:12][CH2:11]O2)[CH:6]=[CH:7][CH:8]=1)#[N:2].Br[C:15]1[CH:20]=[CH:19]C=[CH:17][C:16]=1COCOC>>[B:9]1([C:5]2[CH:4]=[C:3]([CH:8]=[CH:7][CH:6]=2)[C:1]#[N:2])[C:17]2[CH:16]=[CH:15][CH:20]=[CH:19][C:11]=2[CH2:12][O:13]1

Participants

3

Reactant 2

HCID 118459381-Bromo-2-((methoxymethoxy)methyl)benzeneHCID 667383483-(1,3,2-Dioxaborolan-2-yl)benzonitrile

Product 1

HCID 11218256HCID 11218256, compound

Procedure

This was prepared as per the procedure in Example 11, from 2-(3-cyanophenyl)-[1,3,2]-dioxaborolane and 1-bromo-2-((methoxymethoxy)methyl)benzene to afford white crystalline product.

Workup

  1. customto afford white crystalline product

Sources & evidence

ORD record
ord-e03397c6a41c4cf89d78991d62858697
Source dataset
uspto-grants-2008_12
Patent number
US07465836B2

Reaction notes

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