1-Bromo-2-((methoxymethoxy)methyl)benzene → HCID 11413327, compound
Reaction equation
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([B:9]2[O:13][CH2:12][CH2:11]O2)=[CH:5][CH:4]=1)#[N:2].Br[C:15]1[CH:20]=[CH:19]C=[CH:17][C:16]=1COCOC>>[B:9]1([C:6]2[CH:5]=[CH:4][C:3]([C:1]#[N:2])=[CH:8][CH:7]=2)[C:17]2[CH:16]=[CH:15][CH:20]=[CH:19][C:11]=2[CH2:12][O:13]1Participants
3
Procedure
This was prepared as per the procedure in Example 11, from 2-(4-cyanophenyl)-[1,3,2]-dioxaborolane and 1-bromo-2-((methoxymethoxy)methyl)-benzene to afford white crystalline product.
Workup
- customto afford white crystalline product
Sources & evidence
- ORD record
- ord-93a8e314e37f4501b0baf39789605b19
- Source dataset
- uspto-grants-2008_12
- Patent number
- US07465836B2
Reaction notes
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